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Chiral Analysis

Chiral Analysis
  • Author : P.L. Polavarapu
  • Publisher :Unknown
  • Release Date :2018-05-30
  • Total pages :790
  • ISBN : 9780444640284
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Summary : Chiral Analysis: Advances in Spectroscopy, Chromatography and Emerging Methods, Second Edition covers an important area of analytical chemistry of relevance to a wide variety of scientific professionals, including chemistry graduate students, analytical chemists, organic chemists, professionals in the pharmaceutical industry, and others with an interest in chirality and chiral analysis. This thoroughly revised second edition covers several new, important areas of chiral analysis that have emerged since the first edition. Three of the new methods provide higher sensitivity than can be realized with the current methods and are expected to become mainstream applications: cavity based methods offer vastly higher sensitivity than conventional polarimetric methods, microwave chiral detection provides unsurpassed sensitivity for identifying diastereomers, and the rotating electric field method offers a competing new approach for the separation of enantiomers. Another topic, chirality in extraterrestrial life, has not been discussed in any other book and is important for understanding the origin of life. Offers the only book to cover both spectroscopic and separation methods in a single volume Provides an up-to-date and detailed review of the various techniques available, including new techniques that have emerged since the first edition Includes contributions from a range of leading experts in the field, now edited by award-winning chirality researcher Prasad Polavarapu

Chiral Analysis

Chiral Analysis
  • Author : Kenneth W. Busch,Marianna A. Busch
  • Publisher :Unknown
  • Release Date :2011-10-13
  • Total pages :720
  • ISBN : 0080469280
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Summary : Chiral Analysis covers an important area of analytical chemistry of relevance to a wide variety of scientific professionals. The target audience is scientific professionals with an undergraduate background in chemistry or a related discipline, specifically organic chemists, researchers in drug discovery, pharmaceutical researchers involved with process analysis or combinatorial libraries, and graduate students in chemistry. Chapters have been written with the nonspecialist in mind so as to be self-contained. * Broad coverage - spectroscopic and separation methods covered in a single volume * Up-to-date and detailed review of the various techniques available and/or under development in this field * Contributions from leading experts in the field

Capillary Electrophoresis in Chiral Analysis

Capillary Electrophoresis in Chiral Analysis
  • Author : Bezhan Chankvetadze
  • Publisher :Unknown
  • Release Date :1997-12-29
  • Total pages :572
  • ISBN : 0471974153
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Summary : Capillary Electrophoresis in Chiral Analysis Bezhan Chankvetadze Tbilisi State University, Republic of Georgia The application of capillary electrophoresis (CE) to the field of chiral analysis has exploded recently. The advantages of capillary electrophoresis - extremely high peak efficiency, excellent compatibility with biological samples, short analysis time, simplicity, versatility and low cost - are perfect for the accurate measurement of optical purity, increasingly important in the regulation-ruled pharmaceutical industry. Although there have been a number of books on capillary electrophoresis and chiral analysis separately, as yet there has been no dedicated monograph on the application of capillary electrophoresis to chiral analysis. This book bridges the gap. Capillary Electrophoresis in Chiral Analysis charts the evolution of chiral capillary electrophoresis and describes new types of chiral selectors and mechanistic aspects of chiral recognition. While on the one hand, it is an excellent introduction to newcomers, on the other, it is of practical use to experienced researchers in the field wishing to solve a particular separation problem. It includes an alphabetical list of chiral compounds resolved using CE with appropriate references, which any one working in the field will find invaluable.

Analysis of Chiral Organic Molecules

Analysis of Chiral Organic Molecules
  • Author : Peter Schreier,Alexander Bernreuther,Manfred Huffer
  • Publisher :Unknown
  • Release Date :1995-01-01
  • Total pages :348
  • ISBN : 9783110867855
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Summary :

Thin Layer Chromatography in Chiral Separations and Analysis

Thin Layer Chromatography in Chiral Separations and Analysis
  • Author : Teresa Kowalska,Joseph Sherma
  • Publisher :Unknown
  • Release Date :2007-06-22
  • Total pages :436
  • ISBN : 9780849343964
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Summary : Thin layer chromatography (TLC) is well suited for performing enantioseparations for research as well as larger-scale applications. A fast, inexpensive, and versatile separation technique, there are many practical considerations that contribute to its effectiveness. Thin Layer Chromatography in Chiral Separations and Analysis is the first bo

Chiral Recognition in Separation Methods

Chiral Recognition in Separation Methods
  • Author : Alain Berthod
  • Publisher :Unknown
  • Release Date :2010-06-16
  • Total pages :337
  • ISBN : 3642124453
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Summary : What drives a scientist to edit a book on a speci c scienti c subject such as chiral mechanisms in separation methods? Until December 2005, the journal Analytical Chemistry of the American Chemical Society (Washington, DC) had an A-page section that was dedicated to simple and clear presentations of the most recent te- niques or the state of the art in a particular eld or topic. The “A-page” section was prepared for a broad audience of chemists including industrial professionals, s- dents as well as academics looking for information outside their eld of expertise. 1 Daniel W. Armstrong, one of the editors of this journal and a twenty-year+ long friend, invited me to present my view on chiral recognition mechanisms in a simple and clear way in an “A-page” article. In 2006, the “A-page” section was maintained as the rst articles at the beginning of each rst bi-monthly issue but the pagination was no longer page distinguished from the regular research articles published by the journal. During the time between the invitation and the submission, the A-page section was integrated into the rest of the journal and the article appeared as (2006) Anal Chem (78):2093–2099.

Chiral Separation Methods for Pharmaceutical and Biotechnological Products

Chiral Separation Methods for Pharmaceutical and Biotechnological Products
  • Author : Satinder Ahuja
  • Publisher :Unknown
  • Release Date :2011-03-31
  • Total pages :400
  • ISBN : 1118097750
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Summary : Discusses chiral separations and offers guidance for selectingthe optimum method for desired results Chiral separations represent the most intriguing and, by somemeasures, most difficultseparations of chemical compounds. Thisbook provides researchers and students an under-standing of chiralseparations and offers a convenient route to selecting the bestseparation method, saving considerable time and cost in productdevelopment. Considering chiral separations in the biotechnological andpharmaceutical industries, as well as for food applications, Dr.Ahuja provides insights into a broad range of topics. Opening witha broad overview of chiral separations, regulatory considerationsin drug product development, and basic issues in methoddevelopment, the book: Covers a variety of modern methods such as gas chromatography,high performance liquid chromatography, supercritical fluidchromatography, and capillary electrophoresis Deals with the impact of chirality on the biological activity ofsmall and large molecules Provides detailed information on useful chiral stationary phases(CSPs) for HPLC Includes handy information on selection of an appropriate CSP,including mechanistic studies Offers strategies for fast method development with HPLC, SFC,and CE Discusses preparatory methods utilized in the pharmaceuticalindustry With in-depth discussions of the current state of the field aswell as suggestions to assist future developments, ChiralSeparation Methods for Pharmaceutical and BiotechnologicalProducts is an essential text for laboratory investigators,managers, and regulators who are involved in chiral separations inthe pharmaceutical industry, as well as students preparing forcareers in these fields.

Chiral Pollutants

Chiral Pollutants
  • Author : Imran Ali,Hassan Y. Aboul-Enein
  • Publisher :Unknown
  • Release Date :2005-07-15
  • Total pages :368
  • ISBN : 9780470867815
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Summary : Today, among the various chiral discrimination methods, chromatography and capillary electrophoresis techniques have become powerful tools in environmental analysis. Therefore, there is a need to describe the art of the determination of the chiral pollutants in the environmental matrices. This book provides the complete information on the types of the chiral pollutants, their toxicities and methods of determination by chromatography and capillary electrophoresis.

Chiral Separation Techniques

Chiral Separation Techniques
  • Author : Ganapathy Subramanian
  • Publisher :Unknown
  • Release Date :2008-01-08
  • Total pages :641
  • ISBN : 9783527611720
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Summary : Thoroughly revised, with either entirely new or completely updated contents, this is a practical manual for the small and large-scale preparation of enantiomerically pure products. The result is a vital resource for meeting the highest purity standards in the manufacture of chiral pharmaceuticals, food additives and related compounds. All the approaches covered here are highly relevant to modern manufacturing and quality control schemes in the pharmaceutical and biotech industries, addressing the increasingly important issue of drug safety in view of tougher regulatory standards worldwide.

Genetic Analysis of Stereospecific Cleavage of the Chiral Herbicide 2-(2,4-dichlorophenoxy)propionate (dichlorprop) in Delftia Acidovorans MC1

Genetic Analysis of Stereospecific Cleavage of the Chiral Herbicide 2-(2,4-dichlorophenoxy)propionate (dichlorprop) in Delftia Acidovorans MC1
  • Author : Kathleen Marika Schleinitz
  • Publisher :Unknown
  • Release Date :2005
  • Total pages :75
  • ISBN : 9783865376022
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Multidimensional Gas Chromatography for Chiral Analysis

Multidimensional Gas Chromatography for Chiral Analysis
  • Author : Anonim
  • Publisher :Unknown
  • Release Date :2018
  • Total pages :229
  • ISBN : OCLC:1053740908
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Summary : ABSTRACT: Multidimensional gas chromatography (MDGC) is well-established GC method used for a diverse range of applications. Enantioselective MDGC (enantio-MDGC) has been suggested as the method of preference for the separation of extremely overlapping enantiomers. An extensive number of literatures describe enantio-MDGC of polychlorinated biphenyls, essential oils and flavor and fragrance and amino acids were reported. In this review, the applications of MDGC approaches both, heart cutting GC–GC and comprehensive GC × GC in chiral analysis is presented. Since the application of these techniques in this filed is very broad so it will be divided into sections according to the type of the compounds.

An Analysis of Meson Production Utilizing a Chiral SU(3) X SU(3) Phenomenological Lagrangian

An Analysis of Meson Production Utilizing a Chiral SU(3) X SU(3) Phenomenological Lagrangian
  • Author : Leaf Turner
  • Publisher :Unknown
  • Release Date :1969
  • Total pages :242
  • ISBN : WISC:89010950681
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The Analysis of Drugs in Biological Fluids

The Analysis of Drugs in Biological Fluids
  • Author : Joseph Chamberlain
  • Publisher :Unknown
  • Release Date :2018-02-06
  • Total pages :368
  • ISBN : 9781351411431
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Summary : This new edition focuses on a variety of techniques available for the analysis of drugs in biological fluids. Over 150 figures and tables help to describe the latest advances and give examples of their applications. Current chiral analysis methods as well as discussions on the impact of chirality are described. Practical aspects of bioanalytical work, including many examples of laboratory problems not often reported in the scientific literature, are examined in depth.

Pharmaceutical Analysis

Pharmaceutical Analysis
  • Author : David C Lee,Michael L. Webb
  • Publisher :Unknown
  • Release Date :2009-02-12
  • Total pages :384
  • ISBN : 9781405172998
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Summary : The use of analytical sciences in the discovery, development andmanufacture of pharmaceuticals is wide-ranging. From the analysisof minute amounts of complex biological materials to the qualitycontrol of the final dosage form, the use of analytical technologycovers an immense range of techniques and disciplines. This book concentrates on the analytical aspects of drugdevelopment and manufacture, focusing on the analysis of the activeingredient or drug substance. It provides those joining theindustry or other areas of pharmaceutical research with a source ofreference to a broad range of techniques and their applications,allowing them to choose the most appropriate analytical techniquefor a particular purpose. The volume is directed at analytical chemists, industrialpharmacists, organic chemists, pharmaceutical chemists andbiochemists.

Chiral Chromatography

Chiral Chromatography
  • Author : Thomas E. Beesley,Raymond P. W. Scott
  • Publisher :Unknown
  • Release Date :1999-01-26
  • Total pages :522
  • ISBN : 0471974277
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Summary : Chiral Chromatography Thomas E. Beesley Advanced Separation Technologies Inc., Whippany, New Jersey, USA Raymond P. W. Scott Chemistry Department, Georgetown University, Washington DC, USA and Chemistry Department, Birkbeck College, University of London, UK Analytical techniques based on separation processes, such as chromatography and electrophoresis, are finding a growing range of applications in chemical, pharmaceutical and clinical laboratories. The Wiley Separation Science Series provides the analyst in these laboratories with well-focused books covering individual techniques, so that they can be applied more efficiently and effectively to contemporary analytical problems. The different enantiomers of a drug can exhibit widely different physiological activity in degree and nature. As a result, the separation and identification of enantiomers is now a very important analytical problem and chiral chromatography is the natural technique to apply to the resolution of such mixtures. Chiral Chromatography provides the reader with a basic understanding of the nature of chromatographic separations and relates the principles specifically to the separation of enantiomers. The following information is included: * chiral separations involving both gas and liquid chromatography * descriptions of the apparatus used for both techniques * detailed discussion on the retention mechanism that results in chiral selectivity * the structure and synthesis of a wide range of chirally active stationary phases used in both gas and liquid chromatography * preparative applications for large scale purification of enantiomers * applications of capillary electrophoresis and capillary electrochromatography. In addition to the above, a large number of examples of the separation of both commercially and physiologically interesting chiral mixtures are given, as is a detailed discussion on the mechanism of selectivity of each example. Thomas Beesley was founder and is the CEO for a leading manufacturer of chiral stationary phases and has published papers on TLC, HPLC and chiral separations involving cyclodextrins. He has also coauthored papers with Daniel W. Armstrong, an expert on modern cyclodextrin columns. Raymond Scott has worked in the field of separation science for over 40 years and has contributed extensively to the development of both gas and liquid chromatography publishing over 160 papers on the subjects.

Quantitative Analysis of Biospecific Interactions

Quantitative Analysis of Biospecific Interactions
  • Author : Per Lundahl,Andreas Lundqvist,Eva Greijer
  • Publisher :Unknown
  • Release Date :1998
  • Total pages :232
  • ISBN : 9057023784
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Summary : The quantitative analysis of biospecific interactions is an area of increasing importance in the course of going from qualitative descriptions of biological systems to advanced quantitative analysis of molecular events in biological processes. A thorough understanding of the kinetics, equilibria, & dynamics of noncovalent interactions in living material is an essential step forward to connect basic biochemistry with physiology & pharmacology. This book is among the few to cover quantitative biospecific analysis as its sole topic. It provides clear descriptions of state-of-the-art procedures for analysis of equilibria & kinetics of biospecific interactions, with straightforward examples of applications to biochemical problems.

Chiral Separations

Chiral Separations
  • Author : Gerald Gübitz,Martin G. Schmid
  • Publisher :Unknown
  • Release Date :2004
  • Total pages :448
  • ISBN : 9781592596485
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Summary : Prominent experts from around the world detail the chromatographic and electroseparation techniques they have developed for chiral separations on an analytical scale. Described in step-by-step detail to ensure successful experimental results, the procedures are presented as either general methods or as specific applications to substance classes and special compounds, with emphasis on high performance liquid chromatography and capillary electrophoresis techniques, but also including thin layer chromotographic, gas chromatographic, supercritical fluid chromatographic as well as recent electrochromotographic techniques.

Chiral Environmental Pollutants

Chiral Environmental Pollutants
  • Author : R. Kallenborn,H. Hühnerfuss
  • Publisher :Unknown
  • Release Date :2001-01-18
  • Total pages :210
  • ISBN : 3540664238
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Summary : This monograph contains a survey on the role of chirality in ecotoxicological processes. The focus is on environmental trace analysis. Areas such as toxicology, ecotoxicology, synthetic chemistry, biology, and physics are also covered in detail in order to explain the different properties of enantiomers in environmental samples. This monograph delivers a comprehensive survey for environmental trace analysts, analytical chemists, ecotoxicologists, food scientists and experienced lab workers.

Principles and Practice of Bioanalysis

Principles and Practice of Bioanalysis
  • Author : Richard F. Venn
  • Publisher :Unknown
  • Release Date :2000-06-22
  • Total pages :382
  • ISBN : 0748408428
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Summary : Principles and Practice of Bioanalysis provides a guide to the methods available and the techniques currently used in this field. It provides up to the minute information and guidance on the methods and strategy used in developing and running ultra-trace analyses for drugs, metabolites and other substances. The authors writes in an informal and didactic style, offering a logical path through the problems of small molecule (bio)analysis and enables readers to choose appropriate methods of analysis for their needs. Principles and Practice of Bioanalysis provides an overview of analytical methods for analytical scientists within the pharmaceutical industry, research and development, the agrochemical industry, and scientists in the health service, biology and biochemistry. It also gives postgraduate students a useful reference for their research methods.

A Practical Guide to Chiral Analysis

A Practical Guide to Chiral Analysis
  • Author : Louis (Pete) A. Silks, III
  • Publisher :Unknown
  • Release Date :2015-08-24
  • Total pages :448
  • ISBN : 0470455500
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Summary : Written by an acclaimed expert in the field, A Practical Guide to Chiral Analysis provides an entry-level, user-friendly introduction to the subject. Highlighting common methods of chiral analysis used by the practitioner as well as recent advances, the text is destined to become the go-to source for analytical chemists, pharmaceutical scientists, and lab technicians when a chiral analytical process needs to be understood or performed. The author includes an entire chapter on the strategies of choosing the correct method chiral analysis method.

Plant Volatile Analysis

Plant Volatile Analysis
  • Author : Hans F. Linskens,John F. Jackson
  • Publisher :Unknown
  • Release Date :1997-04-16
  • Total pages :266
  • ISBN : 354061589X
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Summary : The book covers a vast array of methods for the analysis of volatile compounds exuded by plants. Some of these volatiles are of great commercial importance, including the aromas of wines and teas, and volatiles in fruits. Other volatiles such as essential oils can be useful for chemotaxonomic purposes, and a chapter on an emerging method, that of chemometric analysis of such data, is included. Isoprene and ammonia rarely find a place in analytical methods presented for plant materials, but methods for these volatiles are described in this book. The volatiles given off by flowers are also included, and in situ headspace analysis of these volatiles is described, a method of potential use for the study of insect-plant interactions.