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Scaling Chemical Processes

Scaling Chemical Processes
  • Author : Jonathan Worstell
  • Publisher :Unknown
  • Release Date :2016-10-27
  • Total pages :186
  • ISBN : 9780128047699
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Summary : Scaling Chemical Processes: Practical Guides in Chemical Engineering is one of a series of short texts that each provides a focused introductory view on a single subject. The full library spans the main topics in the chemical process industries for engineering professionals who require a basic grounding in various related topics. They are ‘pocket publications’ that the professional engineer can easily carry with them or access electronically while working. Each text is highly practical and applied, and presents first principles for engineers who need to get up to speed in a new area fast. The focused facts provided in each guide will help you converse with experts in the field, attempt your own initial troubleshooting, check calculations, and solve rudimentary problems. This book discusses scaling chemical processes from a laboratory through a pilot plant to a commercial plant. It bases scaling on similarity principles and uses dimensional analysis to derive the dimensionless parameters necessary to ensure a successful chemical process development program. This series is fully endorsed and co-branded by the IChemE, and they help to promote the series. Offers practical, short, concise information on the basics to help you get an answer or teach yourself a new topic quickly Includes industry examples to help you solve real world problems Provides key facts for professionals in convenient single subject volumes Discusses scaling chemical processes from a laboratory through a pilot plant to a commercial plant

Scale-up Methodology for Chemical Processes

Scale-up Methodology for Chemical Processes
  • Author : Jean-Paul Euzen,Pierre Trambouze,Jean-Pierre Wauquier
  • Publisher :Unknown
  • Release Date :1993
  • Total pages :240
  • ISBN : 2710806460
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Summary : Having gained considerable experience in process development at the Institut FranCais du PEtrole, the authors present a design framework, a review of the available means of investigation, and several examples illustrating their methodology of industrial process scale up. The salient feature of the book is the fact that it addresses a subject which is vital in view of its economic repercussions, yet relatively unknown in technical and scientific circles, due to the confidentiality surrounding it.Contents: 1. Main guidelines of the methodology. 2. Various types of model. 3. Pilot plants and mock-ups. 4. Experimental techniques. 5. Applications to industrial process development. 6. Conclusions. References. Index.

Pilot Plants and Scale-up of Chemical Processes

Pilot Plants and Scale-up of Chemical Processes
  • Author : P. E. Burke,H. M. S. Patel,L. Powell,R. A. Robinson,R. J. Rowlands,P. E. Sawyer,P. N. Sharratt,J. A. Yates
  • Publisher :Unknown
  • Release Date :1997
  • Total pages :97
  • ISBN : UOM:39015041019434
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Summary : One of the biggest challenges facing today's chemist and chemical engineer is the translation of bench chemistry to the pilot plant. This book provides expert insights into current best practice, and will prove an indispensable manual for all those involved in pilot plant design and scale-up implementation - process chemists, engineers and managers alike. The international expertise of the contributors covers a wide range of topics, and new material covered includes: the removal of heavy metals from effluent, heat flow calorimetry, low temperature processes, good manufacturing practice in pilot plants, design issues, the use of statistical methods in the running of pilot plants. Pilot Plants and Scale-Up of Chemical Processes is a must for all those who are, and wish to remain, expert in the field, providing for the first time in print, a comprehensive and unique perspective of pilot plant production.

Chemical Projects Scale Up

Chemical Projects Scale Up
  • Author : Joe M. Bonem
  • Publisher :Unknown
  • Release Date :2018-05-31
  • Total pages :232
  • ISBN : 9780128137284
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Summary : Chemical Projects Scale Up: How to Go from Laboratory to Commercial covers the chemical engineering steps necessary for taking a laboratory development into the commercial world. The book includes the problems associated with scale up, equipment sizing considerations, thermal characteristics associated with scale up, safety areas to consider, recycling considerations, operability reviews and economic viability. In addition to the process design aspects of commercializing the laboratory development, consideration is given to the utilization of a development in an existing plant. Explains how heat removal for exothermic reactions can be scaled up Outlines how a reactor can be sized from batch kinetic data Discusses how the plant performance of a new catalyst can be evaluated Presents how the economics of a new product/process can be developed Discusses the necessary evaluation of recycling in commercial plants

Scale-up in Chemical Engineering

Scale-up in Chemical Engineering
  • Author : Marko Zlokarnik
  • Publisher :Unknown
  • Release Date :2006-08-21
  • Total pages :296
  • ISBN : 9783527607761
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Summary : Covering the important task of the scale-up of processes from the laboratory to the production scale, this easily comprehensible and transparent book is divided into two sections. The first part details the theoretical principles, introducing the subject for readers without a profound prior knowledge of mathematics. It discusses the fundamentals of dimensional analysis, the treatment of temperature-dependent and rheological material values and scale-up where model systems or not available or only partly similar. All this is illustrated by 20 real-world examples, while 25 exercises plus solutions new to this edition practice and monitor learning. The second part presents the individual basic operations and covers the fields of mechanical, thermal, and chemical process engineering with respect to dimensional analysis and scale-up. The rules for scale-up are given and discussed for each operation. Other additions to this second edition are dimensional analysis of pelleting processes, and a historical overview of dimensional analysis and modeling, while all the chapters have been updated to take the latest literature into account. Written by a specialist with more than 40 years of experience in the industry, this book is specifically aimed at students as well as practicing engineers, chemists and process engineers already working in the field.

Exam Prep Flash Cards for Scaling Chemical Processes

Exam Prep Flash Cards for Scaling Chemical Processes
  • Author : Anonim
  • Publisher :Unknown
  • Release Date :2021
  • Total pages :229
  • ISBN : 1230987654XX
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Summary :

Industrial Process Scale-up

Industrial Process Scale-up
  • Author : Jan Harmsen
  • Publisher :Unknown
  • Release Date :2013-04-25
  • Total pages :112
  • ISBN : 9780444627391
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Summary : This book will help industrial process innovators in research, development and commercial start-up to assess the risks of commercial-scale implementation and provide them with practical guidelines and methods to reduce the risks to acceptable levels. The book can also be used in co-operation with industrial R&D people and academic researchers to shape open innovation programs and in education as a reference book for process innovation courses. Offers easily accessible, step-by-step, and concise guidelines for industrial process scale-up Explains each stage of the innovation funnel: research, development, demonstration, commercial implementation for any process type and branch Based on industrial experiences and practices, which reduces the risks of commercial scale implementation of new processes to acceptable levels and reduces cost and time of process innovation Very clear, attractive layout, using text boxes that contain clarifying notes and additional information on specific topics, which makes it a quick reference of main subjects and additional information

Dimensional Analysis and Scale-up in Chemical Engineering

Dimensional Analysis and Scale-up in Chemical Engineering
  • Author : Marko Zlokarnik
  • Publisher :Unknown
  • Release Date :2012-12-06
  • Total pages :178
  • ISBN : 9783642766732
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Summary : Contemporary Chemical Process Engineers face complex design and research problems. Temperature-dependent physical properties and non-Newtonian flow behavior of substances in a process cannot be predicted by numerical mathematics. Scaling-up equipment for processing can often only be done with partial similarity methods. Standard textbooks often neglect topics like dimensional analysis, theory of similarity and scale-up. This book fills this gap! It is aimed both at university students and the process engineer. It presents dimensional analysis very comprehensively with illustrative examples of mechanical, thermal and chemical processes.

Encyclopedia of Chemical Processing and Design

Encyclopedia of Chemical Processing and Design
  • Author : John J. McKetta Jr
  • Publisher :Unknown
  • Release Date :1994-08-31
  • Total pages :536
  • ISBN : 0824724992
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Summary : "Written by engineers for engineers (with over 150 International Editorial Advisory Board members),this highly lauded resource provides up-to-the-minute information on the chemical processes, methods, practices, products, and standards in the chemical, and related, industries. "

Scaling Analysis in Modeling Transport and Reaction Processes

Scaling Analysis in Modeling Transport and Reaction Processes
  • Author : William B. Krantz
  • Publisher :Unknown
  • Release Date :2007-06-04
  • Total pages :576
  • ISBN : 9780470121924
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Summary : This book is unique as the first effort to expound on the subject of systematic scaling analysis. Not written for a specific discipline, the book targets any reader interested in transport phenomena and reaction processes. The book is logically divided into chapters on the use of systematic scaling analysis in fluid dynamics, heat transfer, mass transfer, and reaction processes. An integrating chapter is included that considers more complex problems involving combined transport phenomena. Each chapter includes several problems that are explained in considerable detail. These are followed by several worked examples for which the general outline for the scaling is given. Each chapter also includes many practice problems. This book is based on recognizing the value of systematic scaling analysis as a pedagogical method for teaching transport and reaction processes and as a research tool for developing and solving models and in designing experiments. Thus, the book can serve as both a textbook and a reference book.

Chemical Process Technology

Chemical Process Technology
  • Author : Jacob A. Moulijn,Michiel Makkee,Annelies E. van Diepen
  • Publisher :Unknown
  • Release Date :2013-03-21
  • Total pages :580
  • ISBN : 9781118570753
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Summary : With a focus on actual industrial processes, e.g. the productionof light alkenes, synthesis gas, fine chemicals, polyethene, itencourages the reader to think “out of the box” andinvent and develop novel unit operations and processes. Reflectingtoday’s emphasis on sustainability, this edition contains newcoverage of biomass as an alternative to fossil fuels, and processintensification. The second edition includes: New chapters on Process Intensification and Processes for theConversion of Biomass Updated and expanded chapters throughout with 35% new materialoverall Text boxes containing case studies and examples from variousdifferent industries, e.g. synthesis loop designs, Sasol I Plant,Kaminsky catalysts, production of Ibuprofen, click chemistry,ammonia synthesis, fluid catalytic cracking Questions throughout to stimulate debate and keep studentsawake! Richly illustrated chapters with improved figures and flowdiagrams Chemical Process Technology, Second Edition is acomprehensive introduction, linking the fundamental theory andconcepts to the applied nature of the subject. It will beinvaluable to students of chemical engineering, biotechnology andindustrial chemistry, as well as practising chemical engineers. From reviews of the first edition: “The authors have blended process technology, chemistryand thermodynamics in an elegant manner… Overall this is awelcome addition to books on chemical technology.”– The Chemist “Impressively wide-ranging and comprehensive… anexcellent textbook for students, with a combination of fundamentalknowledge and technology.” – Chemistry in Britain(now Chemistry World)

Chemical Engineering in the Pharmaceutical Industry

Chemical Engineering in the Pharmaceutical Industry
  • Author : Mary T. am Ende,David J. am Ende
  • Publisher :Unknown
  • Release Date :2019-04-08
  • Total pages :688
  • ISBN : 9781119285502
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Summary : A guide to the important chemical engineering concepts for the development of new drugs, revised second edition The revised and updated second edition of Chemical Engineering in the Pharmaceutical Industry offers a guide to the experimental and computational methods related to drug product design and development. The second edition has been greatly expanded and covers a range of topics related to formulation design and process development of drug products. The authors review basic analytics for quantitation of drug product quality attributes, such as potency, purity, content uniformity, and dissolution, that are addressed with consideration of the applied statistics, process analytical technology, and process control. The 2nd Edition is divided into two separate books: 1) Active Pharmaceutical Ingredients (API’s) and 2) Drug Product Design, Development and Modeling. The contributors explore technology transfer and scale-up of batch processes that are exemplified experimentally and computationally. Written for engineers working in the field, the book examines in-silico process modeling tools that streamline experimental screening approaches. In addition, the authors discuss the emerging field of continuous drug product manufacturing. This revised second edition: Contains 21 new or revised chapters, including chapters on quality by design, computational approaches for drug product modeling, process design with PAT and process control, engineering challenges and solutions Covers chemistry and engineering activities related to dosage form design, and process development, and scale-up Offers analytical methods and applied statistics that highlight drug product quality attributes as design features Presents updated and new example calculations and associated solutions Includes contributions from leading experts in the field Written for pharmaceutical engineers, chemical engineers, undergraduate and graduation students, and professionals in the field of pharmaceutical sciences and manufacturing, Chemical Engineering in the Pharmaceutical Industry, Second Edition contains information designed to be of use from the engineer's perspective and spans information from solid to semi-solid to lyophilized drug products.

Chemical Process Equipment - Selection and Design (Revised 2nd Edition)

Chemical Process Equipment - Selection and Design (Revised 2nd Edition)
  • Author : James R. Couper,W. Roy Penney,James R. Fair, PhD
  • Publisher :Unknown
  • Release Date :2009-08-11
  • Total pages :832
  • ISBN : 0080919723
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Summary : A facility is only as efficient and profitable as the equipment that is in it: this highly influential book is a powerful resource for chemical, process, or plant engineers who need to select, design or configures plant sucessfully and profitably. It includes updated information on design methods for all standard equipment, with an emphasis on real-world process design and performance. The comprehensive and influential guide to the selection and design of a wide range of chemical process equipment, used by engineers globally • Copious examples of successful applications, with supporting schematics and data to illustrate the functioning and performance of equipment Revised edition, new material includes updated equipment cost data, liquid-solid and solid systems, and the latest information on membrane separation technology Provides equipment rating forms and manufacturers’ data, worked examples, valuable shortcut methods, rules of thumb, and equipment rating forms to demonstrate and support the design process Heavily illustrated with many line drawings and schematics to aid understanding, graphs and tables to illustrate performance data

Chemical Processes for a Sustainable Future

Chemical Processes for a Sustainable Future
  • Author : Trevor Letcher,Janet Scott,Darrell Alec Patterson
  • Publisher :Unknown
  • Release Date :2015-11-09
  • Total pages :800
  • ISBN : 9781782621393
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Summary : This comprehensive book approaches sustainability from two directions, the reduction of pollution and the maintaining of existing resources, both of which are addressed in a thorough examination of the main chemical processes and their impact. Divided into five sections, each introduced by a leading expert in the field, the book takes the reader through the various types of chemical processes, demonstrating how we must find ways to lower the environmental cost (of both pollution and contributions to climate change) of producing chemicals. Each section consists of several chapters, presenting the latest facts and opinion on the methodologies being adopted by the chemical industry to provide a more sustainable future. A follow-up to Materials for a Sustainable Future (Royal Society of Chemistry 2012), this book will appeal to the same broad readership - industrialists and investors; policy makers in local and central governments; students, teachers, scientists and engineers working in the field; and finally editors, journalists and the general public who need information on the increasingly popular concepts of sustainable living.

Chemical Reactions and Processes Under Flow Conditions

Chemical Reactions and Processes Under Flow Conditions
  • Author : Santíago V. Luis,Eduardo García-Verdugo,Royal Society of Chemistry (Great Britain)
  • Publisher :Unknown
  • Release Date :2010
  • Total pages :202
  • ISBN : 9780854041923
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Summary : Pharmaceutical and fine chemical products are typically synthesised batchwise which is an anomaly since batch processes have a series of practical and economical disadvantages. On the contrary, flow continuous processes present a series of advantages leading to new ways to synthesise chemical products. Flow processes - * enable control reaction parameters more precisely (temperature, residence time, amount of reagents and solvent etc.), leading to better reproducibility, safer and more reliable processes * can be performed more advantageously using immobilized reagents or catalysts * improve the selectivity and productivity of the process and possibly even the stability of the catalyst * offer opportunities for heat exchange and energy conservation as well as an easy separation and recycling of the reactants and products by adequate process design * achieve multistep syntheses by assembling a line of reactors with minimum or no purification in between two reaction steps * can be assured by facile automation * scale-up can be easily conducted by number-up With all the new research activity in manufacturing chemical products, this comprehensive book is very timely, as it summarises the latest trends in organic synthesis. It gives an insight into flow continuous processes, outlining the basic concepts and explaining the terminology of, and systems approach to, process design dealing with both homogeneous and heterogeneous catalysis and mini- or micro-reactors. The book contains case studies, extensive bibliographies and reference lists in each chapter to enable the reader to grasp the contents and to go on to more detailed texts on specific subjects if desired. The book is written by both organic chemists and engineers giving a multidisciplinary vision of the new tools and methodologies in this field. It is essential reading for organic chemists (in industry or academia) working alongside chemical engineers or who want to undertake chemical engineering projects. It will also be of interest for chemical engineers to see how basic engineering concepts are applied in modern organic chemistry.

Mineral Scales and Deposits

Mineral Scales and Deposits
  • Author : Zahid Amjad,Konstantinos D. Demadis
  • Publisher :Unknown
  • Release Date :2015-05-21
  • Total pages :784
  • ISBN : 9780444627520
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Summary : Mineral Scales and Deposits: Scientific and Technological Approaches presents, in an integrated way, the problem of scale deposits (precipitation/crystallization of sparingly-soluble salts) in aqueous systems, both industrial and biological. It covers several fundamental aspects, also offering an applications’ perspective, with the ultimate goal of helping the reader better understand the underlying mechanisms of scale formation, while also assisting the user/reader to solve scale-related challenges. It is ideal for scientists/experts working in academia, offering a number of crystal growth topics with an emphasis on mechanistic details, prediction modules, and inhibition/dispersion chemistry, amongst others. In addition, technologists, consultants, plant managers, engineers, and designers working in industry will find a field-friendly overview of scale-related challenges and technological options for their mitigation. Provides a unique, detailed focus on scale deposits, includes the basic science and mechanisms of scale formation Present a field-friendly overview of scale-related challenges and technological options for their mitigation Correlates chemical structure to performance Provides guidelines for easy assessment of a particular case, also including solutions Includes an extensive list of industrial case studies for reference

Advanced Control of Chemical Processes 1994

Advanced Control of Chemical Processes 1994
  • Author : D. Bonvin
  • Publisher :Unknown
  • Release Date :2014-05-23
  • Total pages :560
  • ISBN : 9781483297590
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Summary : This publication brings together the latest research findings in the key area of chemical process control; including dynamic modelling and simulation - modelling and model validation for application in linear and nonlinear model-based control: nonlinear model-based predictive control and optimization - to facilitate constrained real-time optimization of chemical processes; statistical control techniques - major developments in the statistical interpretation of measured data to guide future research; knowledge-based v model-based control - the integration of theoretical aspects of control and optimization theory with more recent developments in artificial intelligence and computer science.

Scaling Up

Scaling Up
  • Author : John A. Heitmann
  • Publisher :Unknown
  • Release Date :2005-06
  • Total pages :24
  • ISBN : 0941901017
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Summary : Focusing on petroleum refining and penicillin production. this book is a tribute to the engineers who transformed laboratory reactions into large production facilities. It accompanies CHF's travelling exhibit by the same name.

Pilot Plants and Scale-up of Chemical Processes II

Pilot Plants and Scale-up of Chemical Processes II
  • Author : William Hoyle
  • Publisher :Unknown
  • Release Date :1999
  • Total pages :120
  • ISBN : UOM:39015048550134
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Summary : How do you translate bench chemistry into 10 -100 litre pilot plant scale? Drawing on the wealth of experience of its expert contributors, Pilot Plants and Scale-up of Chemical Processes II provides an insight into how methods, procedures and techniques can be optimised. Up-to-date and highly focused, this book addresses topics including the choice of phase-transfer catalyst, safe scale-up of both Grignard and organolithium reactions, and on-line techniques for examining crystallisation. Newly established collaborative industry/academia projects are discussed, along with other procedures that have a practical application in industry. As a source of innovative techniques and best current practice, this book is a must for process development and pilot plant chemists as well as chemical engineers.

Linear-Scaling Techniques in Computational Chemistry and Physics

Linear-Scaling Techniques in Computational Chemistry and Physics
  • Author : Robert Zaleśny,Manthos G. Papadopoulos,Paul G. Mezey,Jerzy Leszczynski
  • Publisher :Unknown
  • Release Date :2011-03-21
  • Total pages :516
  • ISBN : 9048128536
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Summary : "Linear-Scaling Techniques in Computational Chemistry and Physics" summarizes recent progresses in linear-scaling techniques and their applications in chemistry and physics. In order to meet the needs of a broad community of chemists and physicists, the book focuses on recent advances that extended the scope of possible exploitations of the theory. The first chapter provides an overview of the present state of the linear-scaling methodologies and their applications, outlining hot topics in this field, and pointing to expected developments in the near future. This general introduction is then followed by several review chapters written by experts who substantially contributed to recent developments in this field. The purpose of this book is to review, in a systematic manner, recent developments in linear-scaling methods and their applications in computational chemistry and physics. Great emphasis is put on the theoretical aspects of linear-scaling methods. This book serves as a handbook for theoreticians, who are involved in the development of new efficient computational methods as well as for scientists, who are using the tools of computational chemistry and physics in their research.

Chemical Engineering in the Pharmaceutical Industry, Active Pharmaceutical Ingredients

Chemical Engineering in the Pharmaceutical Industry, Active Pharmaceutical Ingredients
  • Author : David J. am Ende,Mary T. am Ende
  • Publisher :Unknown
  • Release Date :2019-04-23
  • Total pages :1168
  • ISBN : 9781119285861
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Summary : A guide to the development and manufacturing of pharmaceutical products written for professionals in the industry, revised second edition The revised and updated second edition of Chemical Engineering in the Pharmaceutical Industry is a practical book that highlights chemistry and chemical engineering. The book’s regulatory quality strategies target the development and manufacturing of pharmaceutically active ingredients of pharmaceutical products. The expanded second edition contains revised content with many new case studies and additional example calculations that are of interest to chemical engineers. The 2nd Edition is divided into two separate books: 1) Active Pharmaceutical Ingredients (API’s) and 2) Drug Product Design, Development and Modeling. The active pharmaceutical ingredients book puts the focus on the chemistry, chemical engineering, and unit operations specific to development and manufacturing of the active ingredients of the pharmaceutical product. The drug substance operations section includes information on chemical reactions, mixing, distillations, extractions, crystallizations, filtration, drying, and wet and dry milling. In addition, the book includes many applications of process modeling and modern software tools that are geared toward batch-scale and continuous drug substance pharmaceutical operations. This updated second edition: • Contains 30new chapters or revised chapters specific to API, covering topics including: manufacturing quality by design, computational approaches, continuous manufacturing, crystallization and final form, process safety • Expanded topics of scale-up, continuous processing, applications of thermodynamics and thermodynamic modeling, filtration and drying • Presents updated and expanded example calculations • Includes contributions from noted experts in the field Written for pharmaceutical engineers, chemical engineers, undergraduate and graduate students, and professionals in the field of pharmaceutical sciences and manufacturing, the second edition of Chemical Engineering in the Pharmaceutical Industry focuses on the development and chemical engineering as well as operations specific to the design, formulation, and manufacture of drug substance and products.